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Mid Infrared Spectromicroscopy (Mid-IR)

IRsweep

IRis-F1 Dual-comb Spectrometer

🟡 Special Request

The IRsweep IRis-F1 spectrometer uses a dual frequency comb laser source to provide high signal-to-noise measurements with microsecond time resolution.

Contact our Beamline Responsible if you are interested in using this endstation.

This spectrometer is an excellent complement to broadband FT-IR measurements where information about the dynamics of the system of interest is limited by the useful time resolution of rapid-scan measurements or by the reproducibility requirements of step-scan measurements.

Time-Resolved Measurement Modes

There are a number of different measurement modes with implications for time resolution.

Static Measurement

Closest to a traditional FT-IR rapid-scan measurement, but with faster measurement rates and times.

  • Traditional background measurement

  • Sample measurements can be repeated as needed

  • Rapid multiple static acquisition limited by repetition rate / signal-to-noise requirements

    • Example: 1 ms acquisition has minimum 7 ms duty cycle for up to 3.4 s with good noise floor

    • Duty cycle can be specified

    • Measurement can continue indefinitely at reduced duty cycle (256 ms for above 1 ms example)

  • Start of measurement can be triggered

Triggered Static

Same as Static Measurement, except each measurement is controlled externally.

  • Single trigger to collect single measurement

  • Duty cycle and repetition rate are determined by external trigger

Triggered Time-Resolved

Best time resolution, similar to FT-IR step-scan measurement.

  • Background is collected as pre-trigger samples for each repetition

  • Requires a sample system with a reproducible trigger (like step-scan)

  • Finite time window

  • Sample measurement repeated to build S/N (co-addition)

  • Default time resolution is 4 µs, minimum is 1 µs

More Information

Thorlabs website has an introduction to the dual-comb laser technique and advantages: https://www.thorlabs.com/irsweep-dual-comb-spectrometers

irsweep-20260413-152200.jpg
IRsweep IRis-F1 Spectrometer

Techniques

Time-resolved spectroscopy with various sample geometries:

Transmission
Reflection
ATR

 

Schematic

image-20250712-001657.png

Specifications

Center Wavenumber

1650 cm⁻¹

Bandwidth

50 cm⁻¹

Spectral Sampling

0.3 cm⁻¹

Linewidth

<10 MHz (0.0003 cm⁻¹)

Time Resolution

<1 μs